- Type of paper
: Paper in journal
Title: PREPARATIVE ORGANIC PHOTOCHEMISTRY,3. EXPERIMENTAL
TEHCNIQUES
- Authors:
- Bajić, Miroslav (1543)
- Bajić, Marina (193844)
- Karminski-Zamola, Grace (20316)
Journal: KEMIJA U INDUSTRIJI
Number: 1
Volume: 44
Year: 1995
Pages: from 1 to 7
Number of references: 19
Language: hrvatski
Summary: Experimental photochemical techniques, Photochemical
reactors, Light sources, light filters, Solvents. The article reviews
experimental techniques and photochemical apparatus for carrying out
photochemical reactions in preparative organic photochemical laboratories.
Keywords: Preparative organic photochemistry, Experimental techniques
- Type of paper
: Summary in proceedings
Title: PREPARATION OF AROMATIC AND HETEROCYCLIC
BENZO(2,1-b)THIOPHENE-2-CARBOXAMIDES AND THEIR CYCLIZATION BY PHOTOCHEMICAL
DEHYDROCHLORINATION
- Authors:
- Karminski-Zamola, Grace (20316)
- Bajić, Miroslav (1543)
Proceedings title: SINOPSISI
Language: hrvatski
Place: Zagreb
Year: 1991
Pages: from 136 to 136
Meeting: XII. SASTANAK KEMIČARA HRVATSKE
Held: from 02/11/91 to 02/13/91
Summary: Key intermediate in the synthesis of
benzoŠ2,1-bĆthiophene-2-carboxamide is
benzoŠ2,1-bĆthiophene-2-carbonylchloride which was prepared by the reaction
of cinnamic acid or cinnamic aldehyde with SOCl2 near pyridine.
Keywords: BENZO(2,1-b)THIOPHENE-2-CARBOXAMIDE,BENZO(2,1-b)THIOPHENE-2-CARBON YLCHLORIDE,CYCLIZATION,PHOTOCHEMICAL DEHYDROCHLORINATION
- Type of paper
: Summary in proceedings
Title: SYNTHESIS AND PHOTOCHEMICAL BEHAVIOUR OF
5-CARBOMETHOXY-3-CHLORO-N-(p-CHLOROPHENYL)BENZO(1,2-b:4,3-b
)DITHIENO(4,5-b")THIOPHENE-2-CARBOXAMIDE
- Authors:
- Karminski-Zamola, Grace (20316)
- Pavličić, Davorka (177273)
- Bajić, Miroslav (1543)
Proceedings title: ABSTRACTS
Language: engleski
Place: Acireale, Catania(ITALY)
Year: 1991
Pages: from 72 to 72
Meeting: MEDITERRANEAN MEETING ON PHOTOCHEMISTRY
Held: from 10/28/91 to 10/31/91
Summary: The title compound was prepared by multistep synthesis
where in one step was introduced photochemical dehydrocyclization.We are
expected that prepared anilide will react in the last step of the reaction
in sence of photochemical dehydrocyclization.
Keywords: 5-CARBOMETHOXY-3-CHLORO-N-(p-CHLOROPHENYL)BENZOŠ1,2-b:4,3-bĆDITHIE NOŠ4,5-b"ĆTHIOPHENE-2-CARBOXAMIDE, PHOTOCHEMICAL DEHYDROCYCLIZATION, PHOTOCHEMICAL DEHYDROHALOGENATION
- Type of paper
: Summary in proceedings
Title: SYNTHESIS AND PHOTOCHEMICAL BEHAVIOUR OF SOME
N,N-PHENYLEN-BIS-3-CHLOROBENZO(2,1-b)THIOPHENE CARBOXAMIDE
- Authors:
- Crnjak, Andrina
- Bajić, Miroslav (1543)
- Karminski-Zamola, Grace (20316)
Proceedings title: ABSTRACTS
Language: engleski
Place: Leuven, Belgium
Year: 1992
Pages: from 255 to 255
Meeting: 14th IUPAC Symposium on Photochemistry
Held: from 07/19/92 to 07/25/92
Summary: The title compounds were prepared by multistep synthesis.We
are expecting that prepared bis carboxamides will react in sence of
photochemical dehydrohalogenation.
Keywords: N,N-PHENYLEN-BIS-3-CHLOROBENZOŠ2,1-bĆTHIOPHENECARBOXAMIDE, PHOTOCHEMICAL DEHYDROHALOGENATION
- Type of paper
: Summary in proceedings
Title: CRYSTAL AND MOLECULAR STRUCTURE OF
2,5-DI-(E-2-METHOXYCARBONYLSTYRYL)THIOPHENE
- Authors:
- Nagl, A
- Hergold-Brundić, A
- Karminski-Zamola, Grace (20316)
- Bajić, Miroslav (1543)
Proceedings title: SINOPSISI
Language: hrvatski
Place: Zagreb
Year: 1993
Pages: from 46 to 46
Meeting: XIII. SKUP HRVATSKIH KEMIČARA
Held: from 02/08/93 to 02/10/93
Summary: The crystal structure of the title compound was determined
using X-rays.
Keywords: CRYSTAL STRUCTURE,2,5-DI-(E-2-METHOXYCARBONYLSTYRYL)THIOPHENE,X-RAYS
- Type of paper
: Summary in proceedings
Title: SYNTHESIS AND PHOTOCHEMISTRY OF SOME NEW PREPARED
DICARBOXANILIDES:
3,7-DICHLORO-N,N-(p-SUBSTITUTED-PHENYL)BENZO(1,2-b:4,5-b)DITHIOPHENE-2,6-DI
CARBOXAMIDE
- Authors:
- Malešević, Miroslav
- Bajić, Miroslav (1543)
- Karminski-Zamola, Grace (20316)
Proceedings title: SINOPSISI
Language: hrvatski
Place: Zagreb
Year: 1993
Pages: from 106 to 106
Meeting: XIII. SKUP HRVATSKIH KEMIČARA
Held: from 02/08/93 to 02/10/93
Summary: Title compounds were prepared by multistep synthesis
starting from terephtalaldehyde and malonic acid.By the reaction of
photochemical dehydrohalogenation we are expecting the preparation of
corresponding quinolones.
Keywords: DICARBOXANILIDES,3,7-DICHLORO-N,N-(p-SUBSTITUTED-PHENYL)BENZO(1,2- b:4,5-b)DITHIOPHENE-2,6-DICARBOXAMIDE,PHOTODEHYDROHALOGENATION
- Type of paper
: Summary in proceedings
Title: SYNTHESIS AND PHOTOSYNTHESIS OF NEW HETEROPOLYCYCLIC
DIACRYLIC ACID: BENZO(2,1-b:3,4-b )DITHIOPHENE-2,7-DIACRYLIC ACID
- Authors:
- Pavličić, Davorka (177273)
- Karminski-Zamola, Grace (20316)
- Bajić, Miroslav (1543)
Proceedings title: SINOPSISI
Language: hrvatski
Place: Zagreb
Year: 1993
Pages: from 107 to 107
Meeting: XIII. SKUP HRVATSKIH KEMIČARA
Held: from 02/08/93 to 02/10/93
Summary: It was prepared the title compound by multistep synthesis.
Keywords: BENZOŠ2,1-b:3,4-bĆDITHIOPHENE-2,7-DIACRYLIC ACID, PHOTODEHYDROCYCLIZATION
- Type of paper
: Summary in proceedings
Title: PHOTOCHEMICAL REARRANGEMENT OF 5,5 -DIPHENYL-3,3
-DIMETHYL-4,4 -METHYLENEDIISOXAZOLE
- Authors:
- Balent, Zvonimir
- Filipović-Marinić, N
- Karminski-Zamola, Grace (20316)
Proceedings title: SINOPSISI
Language: hrvatski
Place: Zagreb
Year: 1993
Pages: from 111 to 111
Meeting: XIII. SKUP HRVATSKIH KEMIČARA
Held: from 02/08/93 to 02/10/93
Summary: Irradiation of 5,5 -diphenyl-3,3
-dimethyl-4,4-methyleneisoxazole by UV light gave the mixture of isomeres
together with a lot of decomposition products.After isolation on the column
chromatography it was identified 3-methyl-5-phenylisoxazole.
Keywords: PHOTOCHEMICAL REARRANGEMENT, 5,5 -DIPHENYL-3,3 -DIMETHYL-4,4-METHYLENEDIISOXAZOLE, 3-METHYL-5-PHENYLISOXAZOLE
- Type of paper
: Summary in proceedings
Title: MASS SPECTRAL FRAGMENTATION PATTERNS OF SOME NEW PREPARED
HETEROPOLYCYCLIC DIANILIDES AND ANILIDO-QUINOLONES
- Authors:
- Karminski-Zamola, Grace (20316)
- Bajić, Miroslav (1543)
- Dogan, Jasna
Proceedings title: SINOPSISI
Language: hrvatski
Place: Zagreb
Year: 1995
Pages: from 109 to 109
Meeting: XIV SKUP HRVATSKIH KEMIČARA
Held: from 02/06/95 to 02/08/95
Summary: The electron impact mass spectra of some new
heteropolycyclic dianilides and anilidoquinolones are presented.
Keywords: Mass spectra, Dianilides, Anilidoquinolones
- Type of paper
: Summary in proceedings
Title: PHOTOCHEMISTRY OF 2,5-DISTYRYLFURANS AND
2,5-DISTYRYLTHIOPHENES
- Authors:
- Bajić, Miroslav (1543)
- Karminski-Zamola, Grace (20316)
Proceedings title: Book of Abstracts
Language: engleski
Place: Krems, Austria
Year: 1993
Pages: from 50 to 50
Meeting: Central European Photochemistry Conference
Held: from 10/03/93 to 10/06/93
Summary: Oxidative photocyclization of 2,5-di-(E-carboxystyryl)furan
and 2,5-di-(E-2-carboxystyryl)thiophene was investigated.
Keywords: Oxydative photocyclization, 2,5-distyrylfurans, 2,5-dystyrylthiophenes
- Type of paper
: Summary in proceedings
Title: PHOTOSYNTHESIS OF A NEW HETEROPOLYCYCLIC QUINOLONES
- Authors:
- Dogan, Jasna
- Karminski-Zamola, Grace (20316)
Proceedings title: Book of Abstracts
Language: engleski
Place: Prague, Češka republika
Year: 1994
Pages: from 267 to 267
Meeting: XVth IUPAC Symposium on PHOTOCHEMISTRY
Held: from 07/17/94 to 07/22/94
Summary: A new heteropolycyclic quinolones were prepared by
multistep synthesis, where in one step was introduced photochemical
dehydrohalogenation reaction.
Keywords: Quinolones, Photochemical dehydrohalogenation
- Type of paper
: Summary in proceedings
Title: PHOTOSYNTHESIS OF SOME NEW HETEROPOLYCYCLIC QUINOLONES
- Authors:
- Dogan, Jasna
- Karminski-Zamola, Grace (20316)
Proceedings title: SINOPSISI
Language: hrvatski
Place: Zagreb
Year: 1995
Pages: from 122 to 122
Meeting: XIV SKUP HRVATSKIH KEMIČARA
Held: from 02/06/95 to 02/08/95
Summary: Some new heteropolycyclic dianilides are prepared by
photochemical dehydrohalogenation reaction from corresponding
anilidoquinolones.
Keywords: Heteropolycyclic dianilides, Photochemical dehydrohalogenation, Anilidoquinolones
- Type of paper
: Summary in proceedings
Title: SYNTHESIS AND PHOTOSYNTHESIS OF SOME HETEROPOLYCYCLIC
ANILIDES AND QUINOLONES
- Authors:
- Malešević, Miroslav
- Bajić, Miroslav (1543)
- Karminski-Zamola, Grace (20316)
Proceedings title: SINOPSISI
Language: hrvatski
Place: Zagreb
Year: 1995
Pages: from 123 to 123
Meeting: XIV SKUP HRVATSKIH KEMIČARA
Held: from 02/06/95 to 02/08/95
Summary: Some new heteropolycyclic quinolones are prepared by
multistep synthesis including twofold photochemical dehydrohalogenation
reaction of corresponding anilides.
Keywords: Quinolones, Anilides, Photochemical dehydrohalogenation
- Type of paper
: Summary in proceedings
Title: NUCLEIC ACID BINDING OF HETEROARYL DIAMIDES
- Authors:
- Karminski-Zamola, Grace (20316)
- Bajić, Miroslav (1543)
- Malešević, Miroslav
- Howes, R.
- Wilson, D.
- Boykin, David W.
Proceedings title: SINOPSISI
Language: hrvatski
Place: Zagreb
Year: 1995
Pages: from 157 to 157
Meeting: XIV SKUP HRVATSKIH KEMIČARA
Held: from 02/06/95 to 02/08/95
Summary: The compounds 1-3 are prepared as the potential anti-HIV
agents. The Tm values demonstrate that 1 and 2 bind moderately well to
calf thymus DNA and poly dA*dT. The binding of 1 and 2 to poly A*U, model
for RNA, is significant but more modest. Compound 3 fails to bind to both
types of nucleic acids. The values (ca. 0.3) of the slope of log kapp vs -
logŠNa+Ć for 1 and 2 are consistent with that of the naphthlenedimides
(o.3) and different from the classically intercalating dication propidium
(0.56). The results from studies of salt concentrations on cinetics of
binding to DNA clearly demonstrate that both compounds with extensive
planar aromatic cores 1 and 2 are threading intercalators. It is
interesting that compound 3, also a symmetrical diamide does not bind to
either type of nucleic acid. The failure of 3 to bind to DNA can be
explained based upon the non-planar geometry of 3. MM2 calculations predict
that the amide functional group is twisted significanzly from the plane of
the vinyl thiophene unit. Such twisted structures are not expected to
provide good fits to intercalation cavities.
Keywords: Anti-HIV action, Selectivity against RNA-DNA duplex, dTm method
- Type of paper
: Summary in proceedings
Title: SYNTHESIS OF SOME SUBSTITUTED FURYL- AND THIENYLACRYLATES
BY PALLADIUM(II) CATALYSED VINYLATION OF BROMOFURANS AND BROMOTHIOPHENES
- Authors:
- Dogan, Jasna
- Bajić, Miroslav (1543)
- Blažević, Jelena
- Ćaleta, Tonća
- Karminski-Zamola, Grace (20316)
Proceedings title: SINOPSISI
Language: hrvatski
Place: Zagreb
Year: 1995
Pages: from 179 to 179
Meeting: XIV SKUP HRVATSKIH KEMIČARA
Held: from 02/06/95 to 02/08/95
Summary: Some new furyl- and thienylacrilates and acrylic acids are
prepared in good yields by palladium catalysed coupling of substituted
bromofurans and bromothiophenes with ethyl acrylate.
Keywords: Rurylacrilates, Thienylacrilates, Catalytic vinylation, Palladium(II)acetate
- Type of paper
: Summary in proceedings
Title: SYNTHESIS OF SOME DI- AND TETRA-THIOPHENEACRYLATES BY
PALLADIUM(II) CATALYSED VINYLATION OF DIBROMO- AND TETRABROMOTHIOPHENES
- Authors:
- Malešević, Miroslav
- Dogan, Jasna
- Duraj, Danijela
- Karminski-Zamola, Grace (20316)
Proceedings title: SINOPSISI
Language: hrvatski
Place: Zagreb
Year: 1995
Pages: from 180 to 180
Meeting: XIV SKUP HRVATSKIH KEMIČARA
Held: from 02/06/95 to 02/08/95
Summary: Di- and tetrathienylacrylates are prepared in good yields
by palladium catalysed coupling of corresponding dibromo- and
tetrabromothiophenes.
Keywords: Dibromo- and tetrabromothiophenes, Catalytic vinylation, Palladium(II)acetate
- Type of paper
: Summary in proceedings
Title: SYNTHESIS AND FLUORESCENT CHARACTERISTICS OF SOME NEW
BISBENZOTHIAZOLYL COMPOUNDS
- Authors:
- Tralić-Kulenović, Vesna
- Karminski-Zamola, Grace (20316)
- Fišer-Jakić, Lelja
Proceedings title: ABSTRACTS
Language: engleski
Place: Istanbul, Turska
Year: 1995
Pages: from 669 to 669
Meeting: 35th IUPAC Congress
Held: from 08/14/95 to 08/19/95
Summary: Continuing our investigation on the synthesis and
fluorescence properties of 2-aryl- and 2-heteroarylbenzothiazoles, in
present work we synthesized some new compounds of this group. For all new
substances ultraviolet absorption and fluorescence emission spectra were
taken in ethanol and these characteristics have been discussed as a
function of the heteroatom and the position of the benzothiazole ring.
Keywords: Fluorescence properties, Benzothiazoles, Ultraviolet absorption
- Type of paper
: Summary in proceedings
Title: MASS SPECTRAL FRAGMENTATION PATTERNS OF SOME NEW
3,7-DICHLORO-BENZO(1,2-b:4,5-b')DITHIOPHENE-2,6-DICARBONYLDIANILIDE AND
3,5-DICHLORO-DITHIENO(3,2-b:2',3'-d)THIOPHENE-2,6-DICARBONYLDIANILIDES
- Authors:
- Karminski-Zamola, Grace (20316)
- Malešević, Miroslav
- Blažević, Nikola (4041)
- Bajić, Miroslav (1543)
- Boykin, David W.
Proceedings title: ABSTRACTS
Language: engleski
Place: Istanbul, Turska
Year: 1995
Pages: from 795 to 795
Meeting: 35th IUPAC Congress
Held: from 08/14/95 to 08/19/95
Summary: The electron mass spectra of some new dianilides are
discussed.
Keywords: Mass spectra, Dianilides, Cleavage of a C-N and C-C bond
- Type of paper
: M.A.
Title: SYNTHESIS OF SOME NEW DIANILIDES FROM
BENZOŠ1,2-b:4,5-b'ĆDITHIOPHENES AND DITHIENOŠ3,2-b:2',3'-dĆTHIOPHENES
SERIES AND THEIR PHOTOCHEMICAL TRANSFORMATION INTO SIX-MEMBERED
BIS-LACTAMES (DIQUINOLONES)
Faculty: Fakultet kemijskog inženjerstva i tehnologije Sveušilište u Zagrebu
Author: MALEŠEVIĆ MIROSLAV
Date of defense: 06/21/95
Language: hrvatski
Number of pages: 69
Summary: New heteropolycyclic
diquinolones;benzoŠ1,2-b:4,5-b'dithienoŠ2',3',:2",3"-c'
Ć-5,13-N,N'-dimethyl diquinoline-6,14-dione and
dithyenoŠ3,2-b:2',3'-dĆthienylŠ2',3'-c:2",3"-c'Ć-5,10-N,N'-dimethyl
diquinoline-6,9-dione are prepared by twofold
photochemicaldehydrohalogenation reaction of corresponding
benzodithiophenedicarboxdianilides and
dithienothiophenedicarboxdianilides.Mechanism of the twofold photochemical
dehydrohalogenation are discussed. The fragmentation way in the mass
spectra is determuned on the corresponding dianilides from which
diquinolones were prepared.It was noticed C-C cleavage of the another
anilido group.
Keywords: Heteropolycyclic dianilides, Heteropolycyclic diquinolones, twofold photochemical dehydrohalogenation, Mass spectra.